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Статья
2020

New 11-vertex osmacarborane 1,1-(PPh3)2-1-H-3-O(CH2)4-isonido-1,2,4-OsC2B8H9


E. V. BalagurovaE. V. Balagurova, I. A. GodovikovI. A. Godovikov, I. T. ChizhevskyI. T. Chizhevsky
Российский химический вестник
https://doi.org/10.1007/s11172-020-2888-2
Abstract / Full Text

Hydride-containing 1,1-(PPh3)2-1-H-3-O(CH2)4-isonido-1,2,4-OsC2B8H9 osmacarborane bearing a charge-compensated ligand was synthesized via a reaction of the deprotonated form of medium non-icosahedral 5,6-nido-C2B8H12 carborane with (PPh3)3OsCl2 in a THF solution. The structure of this complex was assigned using 1H, 11B/11B{1H}, and 31P{1H} NMR spectroscopy.

Author information
  • A. N. Nesmeyanov Institute of Organoelement Compounds, Russian Academy of Sciences, 28 ul. Vavilova, 119991, Moscow, Russian FederationE. V. Balagurova, I. A. Godovikov & I. T. Chizhevsky
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