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Статья
2022

One-Step Synthesis of a Steel Corrosion Inhibitor, 1-(2-Neononylamidoethyl)-2-neononyl-2-imidazoline


S. O. BondarevaS. O. Bondareva, Yu. I. MurinovYu. I. Murinov
Российский журнал прикладной химии
https://doi.org/10.1134/S1070427222020045
Abstract / Full Text

1-(2-Neononylamidoethyl)-2-neononyl-2-imidazoline was synthesized in one step from diethylenetriamine and neodecanoic acid in 55–60% yield. Its structure was confirmed by data of gas–liquid chromatography, mass spectrometry, and UV, IR, and 13C NMR spectroscopy. As shown by UV spectroscopy, the product is resistant to acid hydrolysis. The kinetics of its base hydrolysis in 50% aqueous isopropanol at 25–75°С and рН 12.5 was studied. The inhibiting effect of 1-(2-neononylamidoethyl)-2-neononyl-2-imidazoline on the corrosion of St3 low-carbon steel in 2.0 М sulfuric acid and in 1.0 and 4.8 М hydrochloric acid was studied; the degree of protection was 90–94%.

Author information
  • Ufa Institute of Chemistry, Ufa Federal Research Center, Russian Academy of Sciences, Ufa, 450054, Bahskortostan, RussiaS. O. Bondareva & Yu. I. Murinov
References
  1. Tyagi, R., Tyagi, V.K., and Pandey, S.K., J. Oleo Sci., 2007, vol. 56, no. 5, pp. 211−222. https://doi.org/10.5650/jos.56.211
  2. Jevremović, I., Singer, M., Nešić, S., and Mišković-Stanković, V., Corros. Sci., 2013, vol. 77, pp. 265−272. https://doi.org/10.1016/j.corsci.2013.08.012
  3. Frolov, V.I., Tr. Ross. Gos. Univ. Nefti Gaza im. I.M. Gubkina, 2009, no. 2, pp. 165−175.
  4. Abbasov, V.M., Mammadova, T.A., Veliyev, K.R., and Kasamanli, K.H., Open J. Synth. Theory Appl., 2015, vol. 4, no. 2, pp. 33−39. https://doi.org/10.4236/ojsta.2015.42004
  5. Watt, M.M., J. Am. Oil Chem. Soc., 1990, vol. 67, no. 12, pp. 993−995. https://doi.org/10.1007/BF02541864
  6. Shamsa, A., Barmatov, E., Hughes, T.L., Hua, Y., Neville, A., and Barker, R., J. Petrol. Sci. Eng., 2021, vol. 208, part B, ID 109235. https://doi.org/10.1016/j.petrol.2021.109235
  7. Wu, Y. and Herrington, Ph.R., J. Am. Oil Chem. Soc., 1997, vol. 74, no. 1, pp. 61–64. https://doi.org/10.1007/s11746-997-0120-2
  8. Martin, J.A. and Valone, F.W., Corrosion, 1985, vol. 41, no. 5, pp. 281−287. https://doi.org/10.5006/1.3582003
  9. Altsybeeva, A.I., Burlov, V.V., Kuzinova, T.M., Palatik, G.F., and Reshetnikov, S.M., Korroz.: Mater., Zashch., 2006, no. 1, pp. 25−31.
  10. Bondareva, S.O., Lisitskii, V.V., Yakovtseva, N.I., and Murinov, Yu.I., Russ. Chem. Bull., 2004, vol. 53, no. 4, pp. 803−807. https://doi.org/10.1023/B:RUCB.0000037846.18796.e8 
  11. Muktiarti, N., Ditama, I., and Soegijonoa, B., AIP Conf. Proc., 2020, vol. 2242, no. 1, pp. 020023-1−020023-6. https://doi.org/10.1063/5.0007980
  12. Yoo, S.H., Kim, Y.W., Chung, K., Baik, S.Y., and Kim, J.S., Corros. Sci., 2012, vol. 59, pp. 42−54. https://doi.org/10.1016/j.corsci.2012.02.011
  13. Tripathy, D. and Mishra, A., J. Appl. Res. Technol., 2017, vol. 15, no. 2, pp. 93−101. https://doi.org/10.1016/j.jart.2016.12.004
  14. Patent RU 2641148 C2, Publ. 2018.
  15. Patent CN 102964306A, Publ. 2012.
  16. Wang, S.F., Furuno, T., and Cheng, Z., J. Wood Sci., 2003, vol. 49, pp. 371−376. https://doi.org/10.1007/s10086-002-0476-8
  17. Bondareva, S.O., Nugumanov, T.R., Nazarov, I.S., and Murinov, Yu.I., Russ. J. Appl. Chem., 2019, vol. 92, no. 11, pp. 1531–1536. https://doi.org/10.1134/S1070427219110107 
  18. Kolomiets, B.S., German, V.K., and Suchkov, V.V., Zh. Prikl. Khim., 1978, vol. 51, no. 5, pp. 1141–1145.
  19. Ivanov, E.S., Ingibitory korrozii v kislykh sredakh (Corrosion Inhibitors in Acid Media), Moscow: Metallurgiya, 1986.
  20. Verma, C., Quraishi, M.A., and Ebenso, E.E., Int. J. Corros. Scale Inhib., 2020, vol. 9, no. 4, pp. 1261–1276. https://doi.org/10.17675/2305-6894-2020-9-4-5
  21. Jovancicevic, V., Ramachandran, S., and Prince, P., Corrosion, 1999, vol. 55, no. 5, pp. 449–455. https://doi.org/10.5006/1.3284006
  22. Rodríguez-Valdez, L.M., Villamisar, W., Casales, M., González-Rodriguez, J.G., Martínez-Villafañe, А., Martinez, L., and Glossman-Mitnik, D., Corros. Sci., 2006, vol. 48, no. 12, pp. 4053–4064. https://doi.org/10.1016/j.corsci.2006.05.036
  23. Gouron, A., Le Mapihan, K., Camperos, S., Al Farra, A., Lair, V., Ringuedé, A., Cassir, M., and Diawara, B., Appl. Surf. Sci., 2018, vol. 456, pp. 437–444. https://doi.org/10.1016/j.apsusc.2018.06.119
  24. Kuznetsov, Y.I., Andreeva, N.P., and Agafonkina, M.O., Russ. J. Electrochem., 2010, vol. 46, no. 5, pp. 560–564. https://doi.org/10.1134/S1023193510050101 
  25. Swathi, P.N., Rasheeda, K., Samshuddin, S., and Alva, V.D., J. Asian Sci. Res., 2017, vol. 7, no. 8, pp. 301–308. https://doi.org/10.18488/journal.2.2017.78.301.308
  26. Rehioui, M., About, S., Benzidia, B., Hammouch, H., Erramli, H., Daoud, N.A., Badrane, N., and Hajjaji, N., Heliyon, 2021, vol. 7, no. 4, ID e06674. https://doi.org/10.1016/j.heliyon.2021.e06674