Synthesis of double ammonium’calcium pyrophosphate monohydrate Ca(NH4)2P2O7•H2O as the p recursor of biocompatible phases of calcium phosphate ceramics
T. V. Safronova, A. S. Kiselev, T. B. Shatalova, Ya. Yu. Filippov, O. T. Gavlina
Российский химический вестник
https://doi.org/10.1007/s11172-020-2735-5
Double calcium’ammonium pyrophosphate monohydrate Ca(NH4)2P2O7•H2O was synthesized as a result of the interaction of calcium carbonate, an aqueous solution containing pyrophosphoric and lactic acids, and ammonia. The synthesized powder turned black after the thermal treatment in a range of 500—700 °C due to amorphous carbon, which is a product of the destruction of the organic nature components present in the prepared powder. After the thermal treatment at 500 °C, the powder is amorphous to X-rays. The phase composition of the powder after the thermal treatment at 600 °C is presented by β-calcium polyphosphate β-Са(PO3)2, while β-calcium polyphosphate β-Ca(PO3)2 and tromelite Ca4P6О19 are observed after the thermal treatment at 700 °C. The calcium phosphate powder colored due to presence of amorphous carbon can be used as a photocured suspension component that increases the resolution in stereolithographic printing of pre-ceramic semifinished products with a specified geometry of the pore space of calcium phosphate ceramic matrices. The synthesized powder of double calcium’ammonium pyrophosphate monohydrate Ca(NH4)2P2O7•H2O can be applied as a precursor of biocompatible phases for the fabrication of calcium phosphate ceramics used in medicine for the treatment of bone tissue defects.
- Department of Chemistry, M. V. Lomonosov Moscow State University, Building 3, 1 Leninskie Gory, 119991, Moscow, Russian FederationT. V. Safronova, A. S. Kiselev, T. B. Shatalova & O. T. Gavlina
- Department of Materials Science, M. V. Lomonosov Moscow State University, Building 73, 1 Leninskie Gory, 119991, Moscow, Russian FederationT. V. Safronova, T. B. Shatalova & Ya. Yu. Filippov
- Institute of Mechanics, M. V. Lomonosov Moscow State University, 1 Michurinskii prosp., 119192, Moscow, Russian FederationYa. Yu. Filippov
- S. M. Danil’chenko, S. N. Danil’chenko, Vіsnik SumDU. Ser. Fіzika, Matematika, Mekhanika [Bull. Sumy Univ. Ser. Math., Phys. Mech.], 2007, No. 2, 33 (in Russian); http://essuir.sumdu.edu.ua’bitstream/123456789/1152/1/3_Danil.pdf.
- S. Pina, V. P. Ribeiro, C. F. Marques, F. R. Maia, T. H. Silva, R. L. Reis, J. M. Oliveira, Materials, 2019, 12, 1824.
- V. N. Mudraya, I. G. Stepanenko, A. S. Shapovalov, Ukr. Zh. Klinich. Labor. Medyts. [Ukr. J. Clin. Labor. Medic.], 2010, 5 No. 1, 52 (in Russian).
- S. Titsinides, G. Agrogiannis, T. Karatzas, Jpn Dent. Sci. Rev., 2019, 55 No. 1, 26.
- P. D. Sarkisov, N. Y. Mikhailenko, E. E. Stroganova, N. V. Buchilin, S. P. Baskov, Glass Ceram., 2012, 69, No. 5—6, 173.
- J. Jeong, J. H. Kim, J. H. Shim, N. S. Hwang, C. Y. Heo, Biomater. Res., 2019, 23, 1, 4.
- T. V. Safronova, V. I. Putlyaev, Inorg. Mater., 2017, 53, 17.
- A. P. Savitskii, Zhidkofaznoe spekanie sistem s vzaimodeistvuyushchimi komponentami [Liquid-Phase Sintering of Systems with Interacting Components], Nauka, Novosibirsk, 1991, 184 pp. (in Russian).
- N. A. Makarov, Glass Ceram., 2006, 63, No. 3—4, 119.
- M. N. Safina, T. V. Safronova, E. S. Lukin, Glass Ceram., 2007, 64, No. 7—8, 238.
- W. Suchanek, M. Yashima, M. Kakihana, M. Yoshimura, Biomaterials, 1997, 18, 923.
- T. F. Safronova, V. I. Putlyaev, Ya. Yu. Filippov, D. S. Larionov, P. V. Evdokimov, A. E. Averina, E. S. Klimashina, V. K. Ivanov, Refract. Ind. Ceram., 2015, 56 No. 1, 43.
- M. Weil, M. Puchberger, J. Schmedt auf der Guenne, J. Weber, Chem. Mater., 2007, 19, 5067.
- G. MacLennan, C. A. Beevers, Acta Crystallogr., 1956, 9, 187.
- B. Boonchom, C. Danvirutai, J. Optoelectron. Biomed. Mater., 2009, No. 1, 115.
- L. E. Jackson, A. J. Wright, Key Eng. Mater., 2005, 284, 71.
- J. Trommer, M. Schneider, H. Worzala, A. N. Fitch, Mater. Sci. Forum, 2000, 321, 374.
- E. H. Brown, W. E. Brown, J. R. Lehr, J. P. Smith, A. W. Frazier, J. Phys. Chem., 1958, 62, 366.
- L. R. Hossner, J. R. Melton, Soil Sci. Soc. Am. J., 1970, 34, 801.
- Y. V. Subbarao, R. Ellis, Soil Sci. Soc. Am. J., 1975, 39, 1085.
- E. H. Brown, J. R. Lehr, J. P. Smith, A. W. Frazier, J. Agr. Food Chem., 1963, 11, 214.
- D. Zobel, N. Ba, Z. Chem., 1969, 9, 433.
- T. V. Safronova, E. A. Mukhin, V. I. Putlyaev, A. V. Knotko, P. V. Evdokimov, T. B. Shatalova, Ya. Yu. Filippov, A. V. Sidorov, E. A. Karpushkin, Ceram. Int., 2017, 43 No. 1, 1310.
- P. Prokupkova, P. Mošner, L. Koudelka, M. Vlček, J. Mater. Sci., 1998, 33, 743.
- L. E. Jackson, B. M. Kariuki, M. E. Smith, J. E. Barralet, A. J. Wright, Chem. Mater., 2005, 17, 4642.
- T. V. Safronova, V. I. Putlyaev, A. V. Knot’ko, V. K. Krut’ko, O. N. Musskaya, S. A. Ulasevich, N. A. Vorob’eva, V. D. Telitsin, Glass and Ceram., 2018, 75, No. 7—8, 279.
- O. B. Dormeshkin, N. I. Vorob’ev, G. Kh. Cherches, A. N. Gavrilyuk, Trudy BGTU. Khim. Tekhn. Neorg. Veshchestv [Workds of BGTU. Chem. Techn. Inorg. Substances], 2008, 1 No. 3, 65 (in Russian).
- O. Dormeshkin, Interactions Between Components of Complex Fertilizers. Chemical and Physico-Chemical Interactions at the Stages of Mixing, Granulating and Drying During their Production, Lap Lambert Academic Publishing, Mauritius, 2019, 57 pp.
- T. Sugama, M. Allan, J. M. Hill, J. Am. Ceram. Soc., 1992, 75, 8, 2076.
- L. Sharma, D. Kiani, K. Honer, J. Baltrusaitis, ACS Sustainable Chem. Eng., 2019, 7, 6802.
- O. D. Philen, J. R. Lehr, Soil Sci. Soc. Am. J., 1967, 31, 196.
- N. T. Andrianov, V. L. Balkevich, A. V. Belyakov, A. S. Vlasov, I. Ya. Guzman, E. S. Lukin, Yu. M. Mosin, B. S. Skidan, Khimicheskaya tekhnologiya keramiki: ucheb. posobie dlya vuzov [Chemical Technology of Ceramics: Manual for Higher Educational Institutions], Ed. I. Ya. Guzman, OOO Rif Stroimaterialy, Moscow, 2012, 496 pp. (in Russian).
- J. W. Halloran, Annu. Rev. Mater. Res., 2016, 46, 19.
- Y. Li, M. Wang, H. Wu, F. He, Y. Chen, S. Wu, J. Eur. Ceram. Soc., 2019, 39, 4921; https://doi.org/10.1016/j.jeurceramsoc.2019.07.035.
- P. V. Evdokimov, Author’s Abstract, Cand. Sci. (Chem.) Thesis, M. V. Lomonosov Moscow State University, Moscow, 2014, 18 pp. (in Russian).
- T. V. Safronova, V. I. Putlyaev, Y. Y. Filippov, S. A. Vladimirova, D. M. Zuev, G. S. Cherkasova, Glass Ceram., 2017, 74, No. 5—6, 185.
- T. V. Safronova, S. A. Kurbatova, T. B. Shatalova, A. V. Knotko, P. V. Yevdokimov, V. I. Putlyayev, Inorg. Mater. Appl. Res., 2017, 8 No. 1, 118.
- T. V. Safronova, G. K. Kazakova, P. V. Yevdokimov, T. B. Shatalova, A. V. Knotko, A. V. Korotkova, V. I. Putlyayev, Inorg. Mater. Appl. Res., 2016, 7 No. 4, 635.
- T. V. Safronova, V. I. Putlyaev, M. D. Andreev, Ya. Yu. Filippov, A. V. Knot’ko, T. B. Shatalova, P. V. Evdokimov, Inorg. Mater., 2017, 53, 859.
- T. V. Safronova, V. I. Putlyaev, A. V. Knot’ko, T. B. Shatalova, V. Yu. Savinova, Inorg. Mater. Appl. Res., 2019, 10, 841.
- A. I. Vulikh, Ionoobmennyi sintez [Ion-Exchange Synthesis], Khimiya, Moscow, 1973, 232 pp. (in Russian).
- ICDD (2010). PDF-4+ 2010 (Database), Ed. S. Kabekkodu, International Centre for Diffraction Data, Newtown Square, PA, USA; available online: http://www.icdd.com’products/pdf2.htm (accessed on 12 August 2019).
- T. V. Safronova, M. A. Shekhirev, V. I. Putlyaev, Y. D. Tret’yakov, Inorg. Mater., 2007, 43, 901.
- T. V. Safronova, A. V. Kuznetsov, S. A. Korneychuk, V. I. Putlyaev, M. A. Shekhirev, Cent. Eur. J. Chem., 2009, 7, 184.
- V. B. Ioffer, Osnovy proizvodstva vodoroda [Foundations of Hydrogen Production], Gos. Nauchno-Tekhn. Gorno-Topl. Lit., Leningrad, 1960, 430 pp. (in Russian).
- I. C. McNeill, H. A. Leiper, Polym. Degrad. Stab., 1985, 11, 267.
- I. C. McNeill, H. A. Leiper, Polym. Degrad. Stab., 1985, 11, 309.
- E. V. Kukueva, V. I. Putlyaev, A. A. Tikhonov, T. V. Safronova, Inorg. Mater., 2017, 53, 212.